Wednesday, July 08, 2015 2:23:05 AM Dab Bongs
nt a bunch of
thallium around the house about like you want to be kicked in the
teeth with a heavy pair of boots.
A further bad aspect of this method is its high cost. 100 grams sell
for $150, and the high molecular weight of the compound means that a
lot of it has to be used to get a moderate amount of product. One
pound of thallium(ni) nitrate is required for a 1-molar batch.
This method can be found in Tetrahedron Letters No. 60, pages
5275-80 (1970). To produce a one mole batch, dissolve one mole of
propenylbenzene in some methanol, and put it into a one-gallon glass
jug. In a beaker, dissolve one mole (448 grams) of thallium(HI) nitrate
trihydrate in methanol. Then pour the thallium solution into the jug
with the propenylbenzene, and stir at room temperature for 5 minutes.
The thallium(I) nitrate formed by the reaction comes out of solution. It is
removed by filtration.
The propenylbenzene has at this point been converted to a ketal.
This is hydrolyzed to the phenylacetone by shaking the filtrate with
about 2000 ml of 1 molar sulfuric acid solution in water for about 5
minutes. The phenylacetone is then extracted out with a couple of
portions of tolulene. This extract is then washed with 5% NaOH
solution, then distilled or purified by conversion to the bisulfite
12 Studies On The Production OfTMA-2
Production of TMA-2, MDA, etc. from the
There are three good methods for converting the phenylacetone to
the psychedelic amphetamine. Choice number one is to use reductive
amination with a hydrogenation bomb with Raney nickel, ammonia
and alcohol solvent. See Journal of the American Chemical Society,
Volume 70, pages 12811-12 (1948). Also see Chem. Abstracts from
1954, column 2097. This gives a yield of about 80% if plenty of
Raney nickel is used. The preferred conditions for use with MDA is a
temperature of 80 C, and a hydrogen pressure of 50 atmospheres.
The drawback to this method is the need for a shaker device for
the bomb, and also a heater. The use of platinum as the catalyst in the
bomb works great when making MDMA, but gives lousy results when
making MDA. There may be a way around this, however, for serious
experimenters. It has been found in experiments with phenylacetone
that a mixture of ammonia and ammonium chloride produces good
yields of amphetamine (50%) when used in a bomb with platinum
catalyst. Methylenedioxyphenylacetone is quite likely to behave
similarly, along with other phenylacetones.
To use this variation, the following materials are placed in the 1.5
liter champagne bottle hydrogenation device described in Chapter 11 of
Secrets of Methamphetamine Manufacture, Third Edition: .5 gram
platinum in 20 ml distilled water. If this platinum is in the form of
PtO2 instead of reduced platinum metal catalyst obtained with
borohydride, the experimenter must now reduce the platinum by
pressurizing the bottle with hydrogen and stirring fo
It's a dirty job but somebody's got to do it
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Adaptation-7 Speeding colonization with more oxygen
Adaptation-8 Removing the cake before 100% colonization
Adaptation-9 Waiting to remove the rice cake
Adaptation-10 Checking out the terrarium before use
Adaptation-11 Use of a high quality cooler for terrarium
Adaptation-12 Use of a humidity gauge in terrarium
Adaptation-13 Use of a tank heater with air pump
Adaptation-14 Plastic wool for finer bubbles
Adaptation-15 Extra terrariums using ultra sonic humidifiers
Adaptation-16 Use of ice-pak to help initiation of pin heads
Adaptation-17 Adding moisture to the rice cake by injection
Adaptation-18 Continued drying of shrooms in storage
Adaptation-19 Circuit modification to ultra sonic humidifier
Adaptation-20 Adding moisture during substrate preparation
Adaptation-21 Use of a timer to control water droplets
Adaptation-22 Use of home made rice flour
Adaptation-23 Lowering of contamination rate by Presterilization
Adaptation-24: Using a 2 1/2 gallon water jug for filtering
Adaptation-25: Contaminate free mushrooms for spore prints
Adaptation-26: Clean spore print from a questionable cap
table of contents.
Adaptation-1: Use of Big Substrate Jars.
Normally, 1/2 pint canning jars are used to prepare the rice cake
cultures. It is possible to use 1 pint canning jars instead. In fact, in
some parts of the country you may have a difficult time finding the
1/2 pint size.
(13 of 39) 5/1/2002 6:54:26 PM
How To Grow Magic Mushrooms The Magic Mushroom Growers Guide (page 4)
The main benefit to using the larger 1 pint size is that more substrate
can be growing mushrooms in your terrarium. The terrariums
described in this report typically will hold 6 or 8 cakes. If you want
more substrate growing mushrooms, one way to accomplish the goal
is to use bigger cakes.
There are several disadvantages to using bigger cakes. First, it takes
several weeks longer for the fungus to colonize the entire cake.
Another disadvantage is that if you suffer from contamination, you
will be throwing out more substrate material. Lastly, you need to
make sure when you construct your terrarium that you leave a few
more inches of space under the drip shield for the cakes to reside.
Since they are taller, they will require the drip shield to be placed
You may notice mushrooms trying to grow inside the jar before the
substrate is 100% colonized. This is not ideal because you are using
up moisture in the cake for something that you won't consume, but it
is a fact of life using the 1 pint jars. It is normal.
Back to preparation and colonization of substrate.
table of contents.
Adaptation-2: Use of a Pressure Cooker to Sterilize.
Normally, most people will elect to use a large kitchen pot to sterilize
the culture jars. A pressure cooker can be used instead. Instead of
letting the substrate jars sit in boiling water for 1 hour, you can place
them in a pressure cooker set to 10 or 15 P.S.I for 20 m
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